3,5-di-tert-butyl salicylaldehyde

3,5-di-tert-butyl salicylaldehyde - Names and Identifiers

Name	3,5-Di-tert-butyl-2-hydroxybenzaldehyde
Synonyms	3,5-DI-TBUTYLSALICYLALDEHYDE 3,5- di Ding JishuiYang Quan 3,5-Di-tert-butylsalicylaldehyde 3,5-di-tert-butyl salicylaldehyde 3, 5-2 tertiary butyl salicylaldehyde 2-Hydroxy-3,5-di-tert-butylbenzaldehyde 3,5-Di-tert-butyl-2-hydroxybenzaldehyde 3,5-DI-TERT-BUTYL-2-HYDROXYBENZALDEHYDE 3,5-Bis(1,1-dimethylethyl)-2-hydroxy-benzaldehyde
CAS	37942-07-7
EINECS	629-676-0
InChI	InChI=1/C15H22O2/c1-14(2,3)11-7-10(9-16)13(17)12(8-11)15(4,5)6/h7-9,17H,1-6H3
InChIKey	RRIQVLZDOZPJTH-UHFFFAOYSA-N

3,5-di-tert-butyl salicylaldehyde - Physico-chemical Properties

Molecular Formula	C15H22O2
Molar Mass	234.33
Density	1.006±0.06 g/cm3(Predicted)
Melting Point	59-61°C(lit.)
Boling Point	277.6±35.0 °C(Predicted)
Flash Point	116.1°C
Solubility	Soluble in DMSO and methanol.
Vapor Presure	0.00266mmHg at 25°C
Appearance	Solid
Color	Off-White to Light Yellow
BRN	1877810
pKa	9.78±0.23(Predicted)
Storage Condition	Keep in dark place,Sealed in dry,Room Temperature
Sensitive	Air Sensitive
Refractive Index	1.527
MDL	MFCD00191998
Physical and Chemical Properties	The product is light yellow to yellow crystalline powder. melting point 58-60°C.
Use	A Schiff base ligand was prepared for use in the enantioselective copper-catalyzed reaction of phenylacetylene to imine. It is also used to prepare chiral oxazolidine.

3,5-di-tert-butyl salicylaldehyde - Risk and Safety

Hazard Symbols	Xi - Irritant
Risk Codes	36/37/38 - Irritating to eyes, respiratory system and skin.
Safety Description	S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing.
WGK Germany	3
HS Code	29124990
Hazard Note	Irritant

3,5-di-tert-butyl salicylaldehyde - Reference Information

introduction	3, 5-di-tert-butylsalicylaldehyde is an organic intermediate, which can be prepared from 2, 4-di-tert-butylphenol through one-step reaction. It has been reported that it can be used to prepare dimethyl ethylenediamine tert-butylphenol and (S,S)-salenCo (II) catalyst.
apply	500mL eggplant bottle to add 2,4-di-tert-butylphenol 50mmol, paraformaldehyde 500mmol, sodium hydroxide 150mmol, triethylamine 100mmol, tetrahydrofuran 100mL, heating reflux stirring reaction at 90 ℃, TLC tracking the reaction process, after the reaction to room temperature. Add hydrochloric acid to the reaction solution, stir, until the reaction solution is clarified and stratified, the aqueous phase is extracted with ethyl acetate, the organic phase is combined, and the saturated salt water is washed, anhydrous sodium sulfate is dried, filtered, and the solvent is removed. Column chromatography (n-hexane: ethyl acetate = 30:1) purification, the product is 10.56g, and the yield is 90.16%.
preparation	500mL eggplant bottle was added with 2,4-50mmol di-tert-butylphenol, 500mmol paraformaldehyde, 150mmol sodium hydroxide, 100mmol triethylamine, 100mL tetrahydrofuran, heated reflux stirring reaction at 90 ℃, TLC followed the reaction process, and dropped to room temperature after the reaction was completed. Add hydrochloric acid to the reaction solution, stir, until the reaction solution is clarified and stratified, the aqueous phase is extracted with ethyl acetate, the organic phase is combined, and the saturated salt water is washed, anhydrous sodium sulfate is dried, filtered, and the solvent is removed. Column chromatography (n-hexane: ethyl acetate = 30:1) purification, the product is 10.56g, and the yield is 90.16%.
Use	Prepare a Schiff base ligand for the enantioselective copper-catalyzed reaction of phenylacetylene to imine. It is also used to prepare chiral oxazolidine.

Last Update：2024-04-09 20:45:29

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3,5-di-tert-butyl salicylaldehyde
氫桂皮醛

3,5-di-tert-butyl salicylaldehyde

3,5-Di-tert-butyl-2-hydroxybenzaldehyde

CAS: 37942-07-7

Molecular Formula: C15H22O2

3,5-di-tert-butyl salicylaldehyde - Names and Identifiers

3,5-di-tert-butyl salicylaldehyde - Physico-chemical Properties

3,5-di-tert-butyl salicylaldehyde - Risk and Safety

3,5-di-tert-butyl salicylaldehyde - Reference Information

Supplier List

3,5-di-tert-butyl salicylaldehyde Request for Quotation

3,5-Di-tert-butyl-2-hydroxybenzaldehyde

CAS: 37942-07-7

Molecular Formula: C15H22O2

3,5-di-tert-butyl salicylaldehyde - Names and Identifiers

3,5-di-tert-butyl salicylaldehyde - Physico-chemical Properties

3,5-di-tert-butyl salicylaldehyde - Risk and Safety

3,5-di-tert-butyl salicylaldehyde - Reference Information

Supplier List

3,5-di-tert-butyl salicylaldehyde